
Before you begin your write-up, develop a check-list of requirements for the
practical and make sure that your submission meets every one. You need to
make sure that every question which you have been directed to address has indeed
been addressed. Go through the check list with the piece of work in front
of you before you submit.
In scientific reporting, truth is of the highest
importance. The truth, the whole truth and nothing but the truth, is
always required. Even a tiny detail, if it is mis-stated, casts doubt on
the whole document. Never claim as your own, work which is someone else's.
If you don't attribute such work, you are implying that it is yours.
The default font supplied by Word is probably not best for a scientific report.
I recommend "Times New Roman". A good report is short and to the point. A
conversational style is not appropriate. A dry detached style is your
goal. Avoid unnecessary words. Do not repeat yourself. The
words, "as I said before" should never appear.
Two general requirements are
- Your write-up must display understanding of what you have been
doing.
- Your use of English must be clear, concise and grammatical.
- You are doing chemistry, so reactions must be described by means of
chemical equations, and the chemical formulas of substances must be included
where appropriate.
The sections suggested below are flexible: depending on the nature of the
experiment, the method, results, discussion and conclusions sections may be
grouped together. For example, the method section might be grouped with
the results section as "Method & Results". In another case, a "Results &
Conclusions" section might be more appropriate, and so on.
Title
Start with a good title. It should express the aim of the experiment (and
so there is no need for a separate "aim" statement). The title given in the
handbook may not be the best title for your report, since it serves a different
purpose. Use the "heading 1" style.
Introduction
The first section is the introduction. Use the "heading 2" style. Set your
experiment in context with some theoretical background.
Apparatus & Materials
List the items of apparatus and the chemicals and solutions that you used.
Include the capacity of each piece of volumetric apparatus, as well as beakers
and flasks. Always state the concentration of a solution (if known), (except in the case of
indicator solutions, which are made up according to standard recipes, usually
0.1%w/v, in water or a mixture of alcohol and water). Include diagrams in
this section. However, only include a diagram when it adds something to
your report. If
standard apparatus is used in standard ways, no diagram is necessary.
Taking good photographs is not easy. Be very careful about incorporating
them in your write-up. Usually a good diagram is much better.
Hazards
Briefly describe any hazards that the materials, apparatus, or what is to be
done with them might involve. Mention fire, explosion, and toxicity
hazards etc. in clear prose. Explain any symbols or abbreviations.
(This latter is generally true.)
Method
Write clearly what you actually did, making clear any deviations from the
schedule. "The contents of flask A were added to the contents of flask B" or "we
(or I) added the contents of flask A to those of B" are acceptable forms.
Forms such as, "Add the contents of flask A to flask B" are not acceptable.
Results
The next section is the results section. Set out your raw results clearly
in tabular form. This section also includes the processing of your
results, and any graphs you produce. Calculations must be explained.
Chromatograms, or diagrams representing them, would be included here. If you include results from other students, you must attribute them. (Give
the surnames and initials of the students involved.)
Discussion
Set your results in context and discuss any meaning that can be extracted from
them. Confine your attention exclusively to your own work in this
section.
Conclusion(s)
What conclusions can you draw from the results of your experiment?
Your focus must be very narrow. You must not make statements which are not
directly connected with your experiment.
What students do wrong
1. You must report what you did. That rules out, "Pipette 5ml..." or "Add
solution A to solution B..." You have to say, "5 ml were pipetted..." or
"Solution A was added to solution B..."
2. When you borrow results from another group, as you may
sometimes
do, you must say so, and say who they came from. For example, "The value
of n was obtained from the work of N. Greene and M. Sanders..."
3. When it says, "Plot A against B," it means A is on the
vertical axis.
4. All observations, calculations, working and graphs must be in the
Results section.
5. The report must be a consistent and orderly body of work.
It should be arranged logically in proper order. It must not contain
irrelevant material such as photocopies of inappropriate passages.
6. Chemical equations and formulae require subscripts and
superscripts. Learn how to do them or use names. E.g.. S2O82- is not
good, learn how to do S2O82-.
Keyboard shortcuts in Word are "ctrl + =" for subscript and "ctrl + shift + ="
for superscript. HTML uses the tags <sup> and <sub> with </sup> and </sub>
7. The Conclusions section should consist of your
conclusions only and must not contain calculations. Conclusions must be based
exclusively on the experiment you have performed. You must make sure that
you include the conclusions that the practical requires. Include
nothing which is not clearly demonstrated by the experiment you have carried
out. Students tend to include general statements of theory which their
experiment does not provide any evidence for. This is very bad.
8. Don't mix up cm with cm3.
9. All calculations must be fully explained, though briefly. The origin
of any values stated must be described. For example, "The value of m was
obtained from the slope of graph 1" and then go on to say how it was obtained.
10. The work must commence with a title. The word
"title" should not appear. The aim of the experiment is best not stated
separately. It should form part of the title.
11. On a graph, you must show all your points. In scientific graphs you should never join points.
Instead you should draw the line suggested by theory, which should pass close to
all your plotted points, but perhaps not through any of them. This is the
line of best fit. Usually it is a
straight line, a trend line in Excel-speak.